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Name	1,1-Hexamethylenehydrazine	EINECS	N/A
CAS No.	5906-35-4	Density	0.984 g/mL at 25 °C(lit.)
PSA	29.26000	LogP	1.37430
Solubility	N/A	Melting Point	86.0-86.5 °C
Formula	C6H14 N2	Boiling Point	165 °C(lit.)
Molecular Weight	114.191	Flash Point	133 °F
Transport Information	N/A	Appearance	N/A
Safety	A poison by ingestion. Mutation data reported. When heated to decomposition it emits toxic vapors of NO_x.	Risk Codes	36/37/38
Molecular Structure		Hazard Symbols	Xi
Synonyms	1H-Azepine,1-aminohexahydro- (7CI,8CI); (Azepan-1-yl)amine; 1,1-Hexamethylenehydrazine;1-Aminoazepane; 1-Aminohexahydro-1H-azepine; 1-Aminohexahydroazepine;1-Aminohexamethyleneimine; 1-Aminohomopiperidine; 1-Aminoperhydroazepine;Hexahydro-1H-azepin-1-amine; N-Aminoazacycloheptane; N-Aminohexahydroazepine;N-Aminohexamethyleneimine; N-Aminohexamethylenimine; N-Aminohomopiperidine; N-Aminoperhydroazepine;NSC 221198; NSC 82329	Article Data	11

1,1-Hexamethylenehydrazine Synthetic route

: 1310-73-2
sodium hydroxide

: (R)-3-aminoazepan-2-one hydrochloride

: 5906-35-4
1-azepanylamine

Conditions

Conditions	Yield
With hydrogenchloride In tetrahydrofuran; water; ethyl acetate	90%

: 629-03-8
1 ,6-dibromohexane

: 7803-57-8
hydrazine hydrate

: 5906-35-4
1-azepanylamine

Conditions

Conditions	Yield
In methanol for 25.5h; Reflux;	45%

: 111-49-9
hexamethylene imine

: 5906-35-4
1-azepanylamine

: 21223-22-3
(CH2)6NNH2*BH3

: 7732-18-5
water

A: 1333-74-0
hydrogen

B: 11113-50-1
boric acid

C: 5906-35-4
1-azepanylamine

Conditions

Conditions	Yield
In water
In water

: 5906-35-4
1-azepanylamine

: 87-13-8
diethyl 2-ethoxymethylenemalonate

: 94621-04-2
(hexahydro-1H azepinyl-1 amino)-3 ethoxycarbonyl-2 propenoate d'ethyle

Conditions

Conditions	Yield
In methanol for 1h; Ambient temperature;	98%

: 1450-14-2
1,1,1,2,2,2-hexamethyldisilane

: 5906-35-4
1-azepanylamine

: 121667-16-1
1-homopiperidine

Conditions

Conditions	Yield
With potassium hydride In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide for 24h; Ambient temperature;	97%

: 611-10-9
2-ethoxycarbonyl-1-cyclopentanone

: 5906-35-4
1-azepanylamine

: (hexahydro-1H-azepinyl-1 amino)-2 ethoxycarbonyl-1 cyclopentene

Conditions

Conditions	Yield
With sodium sulfite In diethyl ether for 24h; Ambient temperature;	95%

: 698-63-5
5-nitrofurane-2-carboxaldehyde

: 5906-35-4
1-azepanylamine

: 1-(5-nitrofurfurylideneamino)azepane

Conditions

Conditions	Yield
for 0.25h; Heating;	94%

: 40398-01-4
2-chloro-6-methylphenyl isocyanate

: 5906-35-4
1-azepanylamine

: 1-Azepan-1-yl-3-(2-chloro-6-methyl-phenyl)-urea

Conditions

Conditions	Yield
In benzene Heating;	92%

: 5906-35-4
1-azepanylamine

: 28556-81-2
2,6-dimethylphenylisocyanate

: 1-Azepan-1-yl-3-(2,6-dimethyl-phenyl)-urea

Conditions

Conditions	Yield
In benzene Heating;	92%

1,1-Hexamethylenehydrazine Chemical Properties

IUPAC Name: Azepan-1-amine
Synonyms : 1-Aminohexahydroazepine ; 1-Azepanamine ; 1H-Azepin-1-amine, hexahydro- ; 1,1-Hexamethylenehydrazine
Product Categories: Heterocyclic Compounds
CAS NO: 5906-35-4
Molecular Formula of 1,1-Hexamethylenehydrazine (CAS NO.5906-35-4) :C₆H₁₄N₂
Molecular Weight of 1,1-Hexamethylenehydrazine (CAS NO.5906-35-4) :114.19
Molecular structure of 1,1-Hexamethylenehydrazine (CAS NO.5906-35-4) :
EINECS: 227-609-6
Index of Refraction:1.478
Surface Tension: 34 dyne/cm
Density: 0.929 g/cm³
Flash Point: 56.1 °C
Enthalpy of Vaporization: 40.2 kJ/mol
Boiling Point: 165.6 °C at 760 mmHg
Vapour Pressure: 1.86 mmHg at 25°C

1,1-Hexamethylenehydrazine Toxicity Data With Reference

Organism	Test Type	Route	Reported Dose (Normalized Dose)	Effect	Source
rat	LDLo	oral	300mg/kg (300mg/kg)		Acute Toxicity Data. Journal of the American College of Toxicology, Part B. Vol. 1, Pg. 93

1,1-Hexamethylenehydrazine Safety Profile

A poison by ingestion. Mutation data reported. When heated to decomposition it emits toxic vapors of NO_x.
Hazard Codes Irritant Xi
Risk Statements 36/37/38
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements 26-36/37/39
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection.
RIDADR UN 1993 3/PG 3
WGK Germany 3
RTECS CM3165000
HazardClass 3.2
PackingGroup III

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