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1,4-Diaminobutane
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Name

1,4-Diaminobutane

 EINECS 203-782-3
CAS No. 110-60-1 Density 0.865 g/cm3
PSA 52.04000 LogP 1.08460
Solubility cell culture medium: 0.16 mg/mL Melting Point 27 °C
Formula C4H12N2 Boiling Point 159.01 °C at 760 mmHg
Molecular Weight 88.1527 Flash Point 51.667 °C
Transport Information UN 2928 6.1/PG 2 Appearance colourless liquid
Safety 16-26-36/37/39-45 Risk Codes 11-21/22-23-34
Molecular Structure Molecular Structure of 110-60-1 (1,4-Diaminobutane) Hazard Symbols FlammableF, ToxicT
Synonyms

Tetramethylenediamine(7CI);1,4-Butylenediamine;1,4-Diamino-n-butane;1,4-Tetramethylenediamine;NSC 60545;Putramine;Putrascine;Putrescin;Putrescine;a,w-Butanediamine;

Article Data 115

1,4-Diaminobutane Synthetic route

333-93-7

putrescine dihydrochloride

110-60-1

1,4-diaminobutane

Conditions
ConditionsYield
With potassium hydroxide In tetrahydrofuran at 20℃; for 12h; Inert atmosphere;95.4%
110-61-2

butanedinitrile

A

616-45-5

2-pyrrolidinon

B

acrylobutyronitril

acrylobutyronitril

C

110-60-1

1,4-diaminobutane

Conditions
ConditionsYield
With rubidium hydroxide; hydrogen; ethylenediamine; RaNi catalyst doped with Fe and Cr, slurry in water In water at 80℃; under 525053 Torr; Product distribution / selectivity;A 3%
B 1%
C 92%
With cesium hydroxide; hydrogen; ethylenediamine; RaNi catalyst doped with Fe and Cr, slurry in water In water at 80℃; under 525053 Torr; Product distribution / selectivity;A 3%
B 5%
C 90%
With sodium hydroxide; hydrogen; ethylenediamine; RaNi catalyst doped with Fe and Cr, slurry in water In water at 80℃; under 525053 Torr; Product distribution / selectivity;A 4%
B 5%
C 85%
2580-71-4

succinaldehyde dioxime

110-60-1

1,4-diaminobutane

Conditions
ConditionsYield
With ammonium formate; zinc In methanol for 0.133333h; Heating;91%
With ammonium formate; magnesium In methanol at 20℃; for 0.833333h;81%
With hydrogenchloride; ethanol; water Hydrogenation.an Platin;
With ethanol; sodium bei Siedehitze;
With sodium amalgam; ethanol; acetic acid at 50 - 60℃;
32754-99-7

4-aminobutyronitrile

110-60-1

1,4-diaminobutane

Conditions
ConditionsYield
With sodium tetrahydroborate; nickel dichloride In ethanol; acetonitrile at 20℃;79%
289-80-5

1,2-diazine

110-60-1

1,4-diaminobutane

Conditions
ConditionsYield
With Cp*Rh(2-(2-pyridyl)phenyl)H; hydrogen In neat (no solvent) at 100℃; under 27361.8 Torr; for 48h; Catalytic behavior; Glovebox;78%
With potassium hydroxide; aluminum nickel for 2.5h;61%
With ethanol; sodium
110-61-2

butanedinitrile

A

123-75-1

pyrrolidine

B

110-60-1

1,4-diaminobutane

Conditions
ConditionsYield
With ammonia; nickel at 140℃; under 80905.8 Torr; Hydrogenation;
110-61-2

butanedinitrile

110-60-1

1,4-diaminobutane

Conditions
ConditionsYield
With cobalt catalyst; ammonia at 120℃; under 62518.2 - 154457 Torr; Hydrogenation;
With Methyl formate; cobalt catalyst at 65 - 85℃; under 102971 - 154457 Torr; Hydrogenation.anschl. Eindampfen mit konz. HCl;
With ethanol; ammonia; nickel at 100℃; under 62518.2 Torr; Hydrogenation;
136918-14-4

phthalimide

110-56-5

1,4-dichlorobutane

110-60-1

1,4-diaminobutane

Conditions
ConditionsYield
With potassium carbonate; N,N-dimethyl-formamide anschl. mit wss. NaOH;
124-04-9

Adipic acid

110-60-1

1,4-diaminobutane

Conditions
ConditionsYield
With chloroform; tris-(2-chloro-ethyl)-amine; sulfuric acid at 40℃;
With chloroform; tris-(2-chloro-ethyl)-amine; sulfuric acid at 40℃;
With chloroform; tris-(2-chloro-ethyl)-amine; sulfuric acid at 40℃;
70-26-8, 348-66-3, 616-07-9, 7006-33-9

2,5-diaminopentanoic acid

110-60-1

1,4-diaminobutane

Conditions
ConditionsYield
durch Einwirkung von Clostridium septicum;
durch Einwirkung von Proteus vulgaris;
durch Einwirkung von Proteus morganii;
durch Einwirkung von Escherichia coli;

1,4-Diaminobutane Chemical Properties

Chemical Name: 1,4-Diaminobutane
IUPAC NAME: Butane-1,4-diamine
CAS No.: 110-60-1
EINECS: 203-782-3
Molecular Formula: C4H12N2
Molecular Weight: 88.15 g/mol
Melting Point: 27 °C
Density: 0.864 g/cm3 
Flash Point: 51.7 °C
Boiling Point: 159 °C at 760 mmHg
Following is the structure of 1,4-Butanediamine (110-60-1):


Product Categories about 1,4-Butanediamine (110-60-1) are alpha,omega-Alkanediamines ; alpha,omega-Bifunctional Alkanes ; Monofunctional & alpha,omega-Bifunctional Alkanes
The chemical synonymous of 1,4-Butanediamine (110-60-1) are 1,4-Butylenediamine ; 1,4-Tetramethylenediamine ; Butylene-1,4-diamine ; H2N(CH2)4NH2 ; Tetramethyldiamine ; RARECHEM AL BW 0068 ; Putrescin ; Putrescine

1,4-Diaminobutane Uses

The major use of 1,4-Butanediamine (110-60-1) is as an intermediate in organic synthesis and it used for the pharmaceutical and biochemical research.

1,4-Diaminobutane Toxicity Data With Reference

1.    

cyt-hmn:hla 2 mmol/L

     JCLLAX    Journal of Cellular Physiology. 78 (1971),217.
2.    

dns-mus:lvr 2 mmol/L

     AMOKAG    Acta Medicia Okayama. 33 (1979),149.
3.    

dni-mus:ast 10 mmol/L

     AMOKAG    Acta Medicia Okayama. 33 (1979),149.
4.    

dni-mus:lvr 20 mmol/L

     AMOKAG    Acta Medicia Okayama. 33 (1979),149.
5.    

orl-mus LDLo:1600 mg/kg

     AECTCV    Archives of Environmental Contamination and Toxicology. 14 (1985),111.
6.    

orl-rbt LDLo:1600 mg/kg

     CRSBAW    Comptes Rendus des Seances de la Societe de Biologie et de Ses Filiales. 83 (1920),481.
7.    

orl-rbt LDLo:1600 mg/kg

     CRSBAW    Comptes Rendus des Seances de la Societe de Biologie et de Ses Filiales. 83 (1920),481.
8.    

scu-rbt LDLo:1 g/kg

     ZEPTAT    Zeitschrift fuer Experimentelle Pathologie und Therapie. 17 (1915),59.
9.    

ivn-rbt LDLo:80 mg/kg

     CRSBAW    Comptes Rendus des Seances de la Societe de Biologie et de Ses Filiales. 83 (1920),481.
10.    

rec-rbt LDLo:400 mg/kg

     CRSBAW    Comptes Rendus des Seances de la Societe de Biologie et de Ses F

1,4-Diaminobutane Consensus Reports

Reported in EPA TSCA Inventory.

1,4-Diaminobutane Safety Profile

Poison by subcutaneous, intravenous, and rectal routes. Moderately toxic by ingestion. An experimental teratogen. Human mutation data reported. When heated to decomposition it emits toxic fumes of NOx. See also 1,3-BUTANEDIAMINE and AMINES.
Hazard Codes:
F: Flammable
T: Toxic
Risk Statements about 1,4-Butanediamine (110-60-1):
R20/21/22 Harmful by inhalation, in contact with skin and if swallowed. 
R34 Causes burns.
Safety Statements about 1,4-Butanediamine (110-60-1):
S26 In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36/37/39 Wear suitable protective clothing, gloves and eye/face protection. 
S45 In case of accident or if you feel unwell, seek medical advice immediately (show the label where possible).
Attentions:
1. Storage: Keep away from sources of ignition. Store in a cool, dry place. Store in a tightly closed container. Corrosives area. Store under nitrogen.
2. Handling: Do not get on skin and clothing. Do not breathe dust, vapor, mist, or gas. Use only in a chemical fume hood.

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