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1,6,7,12-Tetrachloroperylene tetracarboxylic acid dianhydride
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Name

1,6,7,12-Tetrachloroperylene tetracarboxylic acid dianhydride

 EINECS 937-421-2
CAS No. 156028-26-1 Density 1.962 g/cm3
PSA 86.74000 LogP 6.97200
Solubility N/A Melting Point N/A
Formula C24H4Cl4O6 Boiling Point 757.1 °C at 760 mmHg
Molecular Weight 530.104 Flash Point 287.5 °C
Transport Information N/A Appearance N/A
Safety Risk Codes N/A
Molecular Structure Molecular Structure of 156028-26-1 (1,6,7,12-Tetrachloroperylene tetracarboxylic acid dianhydride) Hazard Symbols N/A
Synonyms

1,6,7,12-Tetrachloro-3,4:9,10-perylenetetracarboxylicdianhydride;1,6,7,12-Tetrachloroperylene-3,4:9,10-tetracarboxylic aciddianhydride;1,6,7,12-Tetrachloroperylene-3,4:9,10-tetracarboxylic dianhydride;5,6,12,13-Tetrachloroperylenetetracarboxylic dianhydride;Perylo[3,4-cd:9,10-c'd']dipyran-1,3,8,10-tetrone,5,6,12,13-tetrachloro-;

Article Data 26

1,6,7,12-Tetrachloroperylene tetracarboxylic acid dianhydride Synthetic route

128-69-8

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

156028-26-1

1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

Conditions
ConditionsYield
With sulfuric acid; chlorine at 120℃;99%
With chlorosulfonic acid; iodine at 65℃; for 20h;98%
With chlorosulfonic acid; iodine at 65℃; for 20h;94%

tetrabutyl 1,6,7,12-tetrachloroperylene-3,4,9,10-tetracarboxylate

156028-26-1

1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

Conditions
ConditionsYield
With toluene-4-sulfonic acid In chlorobenzene for 48h; Reflux;87%
128-69-8

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

A

C24H5Cl3O6

B

156028-26-1

1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

Conditions
ConditionsYield
With chlorosulfonic acid; iodine at 70℃; for 5h;
With chlorosulfonic acid; iodine at 60℃; for 20h;A 35 %Spectr.
B 65 %Spectr.
128-69-8

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

A

1,2,6,7,12-pentachloroperylene-3,4,9,10-tetracarboxylic acid bisanhydride

B

C24H2Cl6O6

C

156028-26-1

1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

Conditions
ConditionsYield
With chlorosulfonic acid; iodine at 70℃; for 20h;
128-69-8

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

A

1,2,6,7,12-pentachloroperylene-3,4,9,10-tetracarboxylic acid bisanhydride

B

156028-26-1

1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

Conditions
ConditionsYield
With chlorosulfonic acid; iodine at 70℃; for 10h;
With chlorosulfonic acid; iodine at 70℃; for 20h; Temperature; Time;A 20 %Spectr.
B 80 %Spectr.
With chlorosulfonic acid; iodine at 60℃; for 15h; Temperature; Time; Overall yield = 98 %;
128-69-8

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

A

C24H5Cl3O6

B

1,2,6,7,12-pentachloroperylene-3,4,9,10-tetracarboxylic acid bisanhydride

C

156028-26-1

1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

Conditions
ConditionsYield
With chlorosulfonic acid; iodine at 65℃; for 20h;A 9 %Spectr.
B 7 %Spectr.
C 84 %Spectr.
108-91-8

cyclohexylamine

156028-26-1

1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

156028-27-2

N,N’-dicyclohexyl-1,6,7,12-tetrachloroperylene-3,4:9,10-tetracarboxylic acid bisimide

Conditions
ConditionsYield
With acetic acid In 1-methyl-pyrrolidin-2-one at 90℃; for 11h;100%
With 1-methyl-pyrrolidin-2-one; acetic acid at 85℃; for 8h; Inert atmosphere;92%
at 135℃; for 24h; Inert atmosphere;90%
2450-71-7

Propargylamine

156028-26-1

1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

1419865-47-6

N,N’-bis-propargyl-1,6,7,12-tetrachloroperylene-3,4,9,10-tetracarboxylic diimide

Conditions
ConditionsYield
In isopropyl alcohol at 90℃;100%
In isopropyl alcohol for 24h; Reflux; Inert atmosphere;52.8%
In isopropyl alcohol Reflux;
107-10-8

propylamine

156028-26-1

1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

N,N'-bis-n-propyl-1,6,7,12-tetrachloroperylene-3,4,9,10-tetracarboxdiimide

Conditions
ConditionsYield
In water; butan-1-ol for 8h;99%
In water; isopropyl alcohol at 65℃; for 9h; Temperature; Inert atmosphere;
156028-26-1

1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

2-(3,4,5-tris(dodec-1-yloxy)phenyl)ethylamine

C112H166Cl4N2O10

Conditions
ConditionsYield
With quinoline; zinc(II) acetate dihydrate at 180℃; for 5h; Inert atmosphere;98%

1,6,7,12-Tetrachloroperylene tetracarboxylic acid dianhydride Chemical Properties

Empirical Formula: C24H4Cl4O6
Molecular Weight: 530.097g/mol
Structure of 1,6,7,12-Tetrachloroperylene tetracarboxylic acid dianhydride (CAS NO.156028-26-1):

Index of Refraction: 1.931
Molar Refractivity: 128.74 cm3
Molar Volume: 270.1 cm3
Polarizability: 51.03×10-24cm3
Surface Tension: 103 dyne/cm
Density: 1.962 g/cm3
Flash Point: 287.5 °C
Enthalpy of Vaporization: 110.3 kJ/mol
Boiling Point: 757.1 °C at 760 mmHg
Vapour Pressure: 8.19E-23 mmHg at 25 °C 
SMILES: c1c2c3c(cc(c4c3c(c1Cl)c5c(cc6c7c5c4c(cc7C(=O)OC6=O)Cl)Cl)Cl)C(=O)OC2=O
InChI: InChI=1/C24H4Cl4O6/c25-9-1-5-13-6(22(30)33-21(5)29)2-11(27)17-18-12(28)4-8-14-7(23(31)34-24(8)32)3-10(26)16(20(14)18)15(9)19(13)17/h1-4H
InChIKey: YGRXZLAMYLGXMF-UHFFFAOYAS

1,6,7,12-Tetrachloroperylene tetracarboxylic acid dianhydride Specification

  1,6,7,12-Tetrachloroperylene tetracarboxylic acid dianhydride , its cas register number is 156028-26-1. It also can be called 5,6,12,13-Tetrachloroisochromeno[4',5',6':6,5,10]anthra[2,1,9-def]isochromene-1,3,8,10-tetrone ; Peryleno[10,9-cd:3,4-c'd']dipyran-1,3,8,10-tetrone, 5,6,12,13-tetrachloro- .

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