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Name	2-methoxy-5-sulfamoylbenzoic acid	EINECS	244-789-1
CAS No.	22117-85-7	Density	1.492 g/cm³
PSA	115.07000	LogP	1.82190
Solubility	N/A	Melting Point	220 °C
Formula	C₈H₉NO₅S	Boiling Point	482.5 °C at 760 mmHg
Molecular Weight	231.229	Flash Point	245.6 °C
Transport Information	N/A	Appearance	N/A
Safety	26-36/37/39	Risk Codes	36/37/38
Molecular Structure		Hazard Symbols	Xi
Synonyms	o-Anisicacid, 5-sulfamoyl- (8CI);2-Methoxy-5-sulfonamidobenzoic acid;5-(Aminosulfonyl)-2-methoxybenzoic acid;	Article Data	19

2-methoxy-5-sulfamoylbenzoic acid Synthetic route

: 33045-52-2
methyl 2-methoxy-5-sulfamoyl-benzoate

: 22117-85-7
2-methoxy-5-sulfamoylbenzoic acid

Conditions

Conditions	Yield
With sodium hydroxide In methanol	98.3%
Stage #1: methyl 2-methoxy-5-sulfamoyl-benzoate With sodium hydroxide; water In methanol at 20℃; for 1h; Stage #2: With hydrogenchloride In methanol; water	98.3%
Stage #1: methyl 2-methoxy-5-sulfamoyl-benzoate With sodium hydroxide; water In methanol at 20℃; for 1h; Stage #2: With hydrogenchloride In methanol; water	98.3%

: 51904-91-7
5-chlorosulfonyl-2-anisic acid

: 22117-85-7
2-methoxy-5-sulfamoylbenzoic acid

Conditions

Conditions	Yield
With ammonia In tetrahydrofuran for 0.5h; Ambient temperature;	94.6%
With ammonia

: 579-75-9
2-Methoxybenzoic acid

: 22117-85-7
2-methoxy-5-sulfamoylbenzoic acid

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 84.9 percent / chlorosulfuric acid / 0.67 h / 60 - 70 °C 2: 94.6 percent / NH3 / tetrahydrofuran / 0.5 h / Ambient temperature View Scheme

: 1603-40-3
3-methylpyridin-2-ylamine

: 22117-85-7
2-methoxy-5-sulfamoylbenzoic acid

: C6H8N2*C8H9NO5S

Conditions

Conditions	Yield
In ethanol at 20℃; for 24h;	95%

: 22117-85-7
2-methoxy-5-sulfamoylbenzoic acid

: 6046-93-1
copper(II) acetate monohydrate

: C16H20CuN2O12S2*2H2O

Conditions

Conditions	Yield
In ethanol; water at 20℃; for 72h;	70%

: 22117-85-7
2-methoxy-5-sulfamoylbenzoic acid

: 168828-90-8
(S)-N-[[3-[3-fluoro-4-[4-morpholinyl]phenyl]-2-oxo-5-oxazolidinyl]methyl]amine

: 1390617-37-4
5-(aminosulfonyl)-N-(S)-[[3-[3-fluoro-4-(morpholin-4-yl)phenyl]-2-oxooxazolidin-5-yl]methyl]-2-methoxy benzamide

Conditions

Conditions	Yield
Stage #1: 2-methoxy-5-sulfamoylbenzoic acid With chloroformic acid ethyl ester; triethylamine In dichloromethane at 0 - 20℃; for 0.5h; Stage #2: (S)-N-[[3-[3-fluoro-4-[4-morpholinyl]phenyl]-2-oxo-5-oxazolidinyl]methyl]amine In dichloromethane at 0 - 20℃; for 4h;	55%

: 22117-85-7
2-methoxy-5-sulfamoylbenzoic acid

: 27144-85-0
2-[4-(3-trifluoromethylphenyl)piperazin-1-yl]ethan-1-amine

: N-<2-<4-(3-trifluoromethylphenyl)-1-piperazinyl>ethyl>2-methoxy-5-methyl sulfamoylbenzamide

Conditions

Conditions	Yield
With triethylamine; isobutyl chloroformate In 1,4-dioxane for 6h; Ambient temperature;	40%

: 22117-85-7
2-methoxy-5-sulfamoylbenzoic acid

: 101403-17-2
2--5-methoxytetralin

: 2-methoxy-N-{2-[(5-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-propyl-amino]-ethyl}-5-sulfamoyl-benzamide

Conditions

Conditions	Yield
With chloroformic acid ethyl ester; triethylamine In acetone at 0℃; for 2h;	32%

: 22117-85-7
2-methoxy-5-sulfamoylbenzoic acid

: 328-74-5
3,5-Bis-(trifluoromethyl)aniline

: 439146-22-2
N-[3,5-bis(trifluoromethyl)phenyl]-2-methoxy-5-sulfamoyl-benzamide

Conditions

Conditions	Yield
	24.2%

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 22117-85-7
2-methoxy-5-sulfamoylbenzoic acid

: 75513-55-2
N-hydroxysuccinimido diphenyl phosphate

: 74402-54-3
N-ethyl-2-aminomethylpyrrole

: 15676-16-1
N-[(1-ethyl-2-pyrrolidinyl)methyl]-2-methoxy-5-sulfamoylbenzamide

Conditions

Conditions	Yield
With triethylamine In acetonitrile	24%

2-methoxy-5-sulfamoylbenzoic acid Chemical Properties

Chemical Name: 2-Methoxy-5-sulfamoylbenzoic acid
IUPAC NAME: 2-methoxy-5-sulfamoylbenzoic acid
CAS No.: 22117-85-7
EINECS: 244-789-1
Molecular Formula: C₈H₉NO₅S
Molecular Weight: 231.23g/mol
Structure:

The synonyms of 2-methoxy-5-sulfamoylbenzoic acid(22117-85-7): 5-sulphamoyl-o-anisic acid;2-Methoxy-5-Sufamoyl Benzoic Acid;5-Aminosulfonyl-2-Methoxybenzoic Acid;5-(Aminosulphonyl)-2-methoxybenzoic acid;2-METHOXY-5-SULFAMOYLBENZOIC ACID;2-METHOXY-5-SULFONYLBENZOIC ACID;2-METHOXY-5-SULPHAMOYLBENZOIC ACID;3-CARBOXY-4-METHOXY-BENZENE SULFONAMIDE;
Density: 1.492 g/cm³
Flash Point: 245.6 °C
Boiling Point: 482.5 °C at 760 mmHg

2-methoxy-5-sulfamoylbenzoic acid Uses

Used as intermediates in organic synthesis and sulpiride intermediates.

2-methoxy-5-sulfamoylbenzoic acid Safety Profile

Hazard Codes:
Xi Irritant

Risk Statements about 2-methoxy-5-sulfamoylbenzoic acid(22117-85-7):
    R36/37/38 Irritating to eyes, respiratory system and skin.
Safety Statements about 2-methoxy-5-sulfamoylbenzoic acid(22117-85-7):
    S26 In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
    S36/37/39 Wear suitable protective clothing, gloves and eye/face protection.

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