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Cas Database |
| Name |
3,3',4',5-Tetrachlorosalicylanilide |
EINECS | 214-576-8 |
| CAS No. | 1154-59-2 | Density | 1.636 g/cm3 |
| PSA | 49.33000 | LogP | 5.33110 |
| Solubility | N/A | Melting Point |
162ºC |
| Formula | C13H7 Cl4 N O2 | Boiling Point | 408.1ºC at 760 mmHg |
| Molecular Weight | 351.016 | Flash Point | 200.6 ºC |
| Transport Information | N/A | Appearance | N/A |
| Safety | Poison by ingestion. A skin irritant. When heated to decomposition it emits very toxic fumes of Cl− and NOx. | Risk Codes | 22 |
| Molecular Structure |
|
Hazard Symbols |
 Xn
|
| Synonyms |
Salicylanilide,3,3',4',5-tetrachloro- (6CI,7CI,8CI); 3,3',4',5-Tetrachlorosalicylanilide;3,5,3',4'-Tetrachlorosalicylanilide;3,5-Dichloro-N-(3,4-dichlorophenyl)-2-hydroxybenzamide; 3,5-Dichlorosalicylicacid 3,4-dichloroanilide; Impregon; Irgasan BS 200; Lenigron; WR 593 |
Article Data | 3 |
3,3',4',5-Tetrachlorosalicylanilide Synthetic route
- 320-72-9
3,5-dichlorosalicylic acid
- 95-76-1
m,p-dichloroaniline
- 1154-59-2
3,3',4',5-tetrachlorosalicylanilide
| Conditions | Yield |
|---|---|
| With phosphorus trichloride In chlorobenzene for 3h; Heating; | 92% |
- 39614-80-7
3,5-dichloro-2-hydroxy-benzoyl chloride
- 95-76-1
m,p-dichloroaniline
- 1154-59-2
3,3',4',5-tetrachlorosalicylanilide
| Conditions | Yield |
|---|---|
| In 1,4-dioxane at 85℃; for 2h; |
- 1154-59-2
3,3',4',5-tetrachlorosalicylanilide
- 541-41-3
chloroformic acid ethyl ester
- 92030-30-3
6,8-dichloro-3-(3,4-dichloro-phenyl)-benzo[e][1,3]oxazine-2,4-dione
| Conditions | Yield |
|---|---|
| In pyridine for 1h; Heating; | 62% |
| With pyridine In acetonitrile |
3,3',4',5-Tetrachlorosalicylanilide Chemical Properties
IUPAC Name: 3,5-Dichloro-N-(3,4-dichlorophenyl)-2-hydroxybenzamide
Synonyms of 3,3',4',5-Tetrachlorosalicylanilide (CAS NO.1154-59-2) : Benzamide, 3,5-dichloro-N-(3,4-dichlorophenyl)-2-hydroxy- ; 3,3',4',5-Tetrachlorosalicylanilide ; 3,5,3',4'-Tetrachlorosalicylanilide
CAS NO: 1154-59-2
Molecular Formula :C13H7Cl4NO2
Molecular Weight :351.0122
Molecular Structure :
Index of Refraction: 1.693
Surface Tension: 63.4 dyne/cm
Density: 1.636 g/cm3
Flash Point: 200.6 °C
Enthalpy of Vaporization: 68.58 kJ/mol
Boiling Point: 408.1 °C at 760 mmHg
Vapour Pressure: 3.03E-07 mmHg at 25°C
Melting point: 162 °C
Appearance: 3,3',4',5-Tetrachlorosalicylanilide (CAS NO.1154-59-2) is off-white to beige crystalline powder.
3,3',4',5-Tetrachlorosalicylanilide Uses
3,3',4',5-Tetrachlorosalicylanilide (CAS NO.1154-59-2) is used as intermediate in organic synthesis .
3,3',4',5-Tetrachlorosalicylanilide Toxicity Data With Reference
| Organism | Test Type | Route | Reported Dose (Normalized Dose) | Effect | Source |
|---|---|---|---|---|---|
| rat | LD50 | oral | 243mg/kg (243mg/kg) | Pesticide Chemicals Official Compendium, Association of the American Pesticide Control Officials, Inc., 1966. Vol. -, Pg. 618, 1966. |
3,3',4',5-Tetrachlorosalicylanilide Consensus Reports
Reported in EPA TSCA Inventory.
3,3',4',5-Tetrachlorosalicylanilide Safety Profile
Poison by ingestion. A skin irritant. When heated to decomposition it emits very toxic fumes of Cl− and NOx.
Hazard Codes
Xn
Risk Statements 22-36/37/38
R22:Harmful if swallowed.
R36/37/38:Irritating to eyes, respiratory system and skin.
3,3',4',5-Tetrachlorosalicylanilide Specification
General Information: As in any fire, wear a self-contained breathing apparatus in pressure-demand, MSHA/NIOSH (approved or equivalent), and full protective gear.
Extinguishing Media: Use water spray, dry chemical, carbon dioxide, or chemical foam.
Handling: Avoid breathing dust, vapor, mist, or gas. Avoid contact with skin and eyes. Avoid ingestion and inhalation.
Storage: Store in a cool, dry place. Store in a tightly closed container.
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