Welcome to LookChem.com Sign In|Join Free
  • or
Home > Products >  > 

Acetamide,2-chloro-N-(2,6-dichlorophenyl)-N-phenyl-

Related Products

Hot Products

Name

Acetamide,2-chloro-N-(2,6-dichlorophenyl)-N-phenyl-

EINECS 239-350-6
CAS No. 15308-01-7 Density 1.411 g/cm3
PSA 20.31000 LogP 4.89690
Solubility N/A Melting Point 143-145 °C
Formula C14H10Cl3NO Boiling Point 487.5 °C at 760 mmHg
Molecular Weight 314.599 Flash Point 248.6 °C
Transport Information N/A Appearance White to off white crystalline powder
Safety Risk Codes N/A
Molecular Structure Molecular Structure of 15308-01-7 (2-chloro-N-(2,6-dichlorophenyl)-N-phenylacetamide) Hazard Symbols N/A
Synonyms

Acetanilide,2,2',6'-trichloro-N-phenyl- (8CI);2,2',6'-Trichloro-N-phenylacetanilide;N-(Chloroacetyl)-2,6-dichlorodiphenylamine;N-(2,6-Dichlorophenyl)-2-chloro-N-phenylacetamide;N-(2,6-Dichlorophenyl)-N-phenylchloroacetamide;2,2',6'-Trichloro-N-phenylacetanilide;2-Chloro-N-(2,6-dichlorophenyl)-N-phenylacetamide;

Article Data 8

Acetamide,2-chloro-N-(2,6-dichlorophenyl)-N-phenyl- Synthetic route

15307-93-4

N-phenyl-2,6-dichloroaniline

79-04-9

chloroacetyl chloride

15308-01-7

2-chloro-N-(2',6'-dichlorophenyl)-N-phenylacetamide

Conditions
ConditionsYield
at 106 - 110℃; for 2h; Acetylation;86%
for 16h; Heating;66%
for 5h; Reflux;
for 5h; Reflux;
In toluene at 120℃; for 3h; Solvent;
3776-30-5

2,2,6,6-tetrachlorocyclohexanone

15308-01-7

2-chloro-N-(2',6'-dichlorophenyl)-N-phenylacetamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 99 percent / TiCl4 / toluene / 2 h / 20 °C
2: Et3N / dimethylformamide / 5 h / 95 - 100 °C
3: 86 percent / 2 h / 106 - 110 °C
View Scheme
62-53-3

aniline

Wang resin-bound styrene 4

Wang resin-bound styrene 4

15308-01-7

2-chloro-N-(2',6'-dichlorophenyl)-N-phenylacetamide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 99 percent / TiCl4 / toluene / 2 h / 20 °C
2: Et3N / dimethylformamide / 5 h / 95 - 100 °C
3: 86 percent / 2 h / 106 - 110 °C
View Scheme
123066-65-9

N-phenyl-2,2,6,6-tetrachlorocyclohexaneimine

15308-01-7

2-chloro-N-(2',6'-dichlorophenyl)-N-phenylacetamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Et3N / dimethylformamide / 5 h / 95 - 100 °C
2: 86 percent / 2 h / 106 - 110 °C
View Scheme
15308-01-7

2-chloro-N-(2',6'-dichlorophenyl)-N-phenylacetamide

15362-40-0

1-(2,6-dichlorophenyl)indolin-2-one

Conditions
ConditionsYield
With aluminium trichloride at 160℃; for 2h;75.4%
With aluminum (III) chloride at 160℃; for 2h;62%
With aluminum (III) chloride at 160℃; for 2h;
With triethylamine hydrochloride-aluminum trichloride at 20 - 60℃; for 4.5h; Reagent/catalyst;
15308-01-7

2-chloro-N-(2',6'-dichlorophenyl)-N-phenylacetamide

15307-79-6

diclofenac sodium

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 75.4 percent / AlCl3 / 2 h / 160 °C
2: 93 percent / 2 N NaOH / ethanol; H2O / 4 h / Heating
View Scheme
15308-01-7

2-chloro-N-(2',6'-dichlorophenyl)-N-phenylacetamide

1146981-11-4

1-{[(2,6-dichlorophenyl)-3-(4-chlorophenyl)]methylene}-1,3-dihydroindol-2-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: aluminum (III) chloride / 2 h / 160 °C
2: piperidine / ethanol / Reflux; Inert atmosphere
View Scheme
15308-01-7

2-chloro-N-(2',6'-dichlorophenyl)-N-phenylacetamide

1146981-16-9

1-{[(2,6-dichlorophenyl)-3-(4-fluorophenyl)]methylene}-1,3-dihydroindol-2-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: aluminum (III) chloride / 2 h / 160 °C
2: piperidine / ethanol / Reflux; Inert atmosphere
View Scheme
15308-01-7

2-chloro-N-(2',6'-dichlorophenyl)-N-phenylacetamide

1146981-19-2

1-{[(2,6-dichlorophenyl)-3-(4-hydroxyphenyl)]methylene}-1,3-dihydroindol-2-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: aluminum (III) chloride / 2 h / 160 °C
2: piperidine / ethanol / Reflux; Inert atmosphere
View Scheme
15308-01-7

2-chloro-N-(2',6'-dichlorophenyl)-N-phenylacetamide

145253-61-8

1-{[(2,6-dichlorophenyl)-3-(4-(dimethylamino)phenyl)]methylene}-1,3-dihydroindol-2-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: aluminum (III) chloride / 2 h / 160 °C
2: piperidine / ethanol / Reflux; Inert atmosphere
View Scheme

Acetamide,2-chloro-N-(2,6-dichlorophenyl)-N-phenyl- Specification

The Acetamide,2-chloro-N-(2,6-dichlorophenyl)-N-phenyl-, with the CAS registry number 15308-01-7, is also known as N-(2,6-Dichlorophenyl)-2-chloro-N-phenylacetamide. Its EINECS number is 239-350-6. This chemical's molecular formula is C14H10Cl3NO and molecular weight is 314.59. What's more, its systematic name is 2-chloro-N-(2,6-dichlorophenyl)-N-phenylacetamide.

Physical properties of Acetamide,2-chloro-N-(2,6-dichlorophenyl)-N-phenyl- are: (1)ACD/LogP: 3.09; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): 3.08; (4)ACD/LogD (pH 7.4): 3.08; (5)ACD/BCF (pH 5.5): 130.17; (6)ACD/BCF (pH 7.4): 130.17; (7)ACD/KOC (pH 5.5): 1135.48; (8)ACD/KOC (pH 7.4): 1135.48; (9)#H bond acceptors: 2; (10)#H bond donors: 0; (11)#Freely Rotating Bonds: 3; (12)Polar Surface Area: 20.31 Å2; (13)Index of Refraction: 1.633; (14)Molar Refractivity: 79.63 cm3; (15)Molar Volume: 222.9 cm3; (16)Polarizability: 31.56×10-24cm3; (17)Surface Tension: 52 dyne/cm; (18)Density: 1.411 g/cm3; (19)Flash Point: 248.6 °C; (20)Enthalpy of Vaporization: 75.34 kJ/mol; (21)Boiling Point: 487.5 °C at 760 mmHg; (22)Vapour Pressure: 1.18E-09 mmHg at 25°C.

Preparation of Acetamide,2-chloro-N-(2,6-dichlorophenyl)-N-phenyl-: this chemical can be prepared by chloroacetyl chloride and 2,6-dichloro-N-phenylaniline at the temperature of 106 - 110 °C. The reaction time is 2 hours. It's a reaction of acetylation. The yield is abou 86%.

Acetamide,2-chloro-N-(2,6-dichlorophenyl)-N-phenyl- can be prepared by chloroacetyl chloride and 2,6-dichloro-N-phenylaniline at the temperature of 106 - 110 °C

Uses of Acetamide,2-chloro-N-(2,6-dichlorophenyl)-N-phenyl-: it can be used to produce 1-(2,6-dichlorophenyl)-1,3-dihydro-2H-indol-2-one at the temperature of 160 °C. It will need reagent AlCl3 with the reaction time of 2 hours. The yield is about 75.4%.

Acetamide,2-chloro-N-(2,6-dichlorophenyl)-N-phenyl- can be used to produce 1-(2,6-dichlorophenyl)-1,3-dihydro-2H-indol-2-one at the temperature of 160 °C

You can still convert the following datas into molecular structure:
(1)Canonical SMILES: C1=CC=C(C=C1)N(C2=C(C=CC=C2Cl)Cl)C(=O)CCl
(2)InChI: InChI=1S/C14H10Cl3NO/c15-9-13(19)18(10-5-2-1-3-6-10)14-11(16)7-4-8-12(14)17/h1-8H,9H2
(3)InChIKey: BPEUHDIEZQWRGC-UHFFFAOYSA-N

Post a RFQ

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

1

What can I do for you?
Get Best Price

Get Best Price for 15308-01-7