- A double ( alkane oxygen silicon-based ) alkane preparation method (by machine translation)
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The invention belongs to the field of organic synthesis reaction, in particular to using trialkoxysilane with dienes as raw material for preparing double ( alkane oxygen silicon-based ) alkane method. The method includes the general formula II compound and general formula III compound in the solvent, the catalyst, to carry out addition reaction of silicon with hydrogen compound of general formula I, the catalyst as a twelve-carbonyl three rutheniums, wherein R is C 1-C 5 alkyl, n is 4, 5, 6, 7, 8, 9 or 10. The method provided by the invention the reaction under normal pressure, with a simple and easy process, the product has high purity, raw materials are apt, mild reaction, the reaction speed is fast, low cost of raw materials, and the like, as the twelve carbonyl three rutheniums catalytic hydrosilylation addition, the traditional Pt compared series catalyst with high selectivity, low price, it is simple to synthesize, and the like. (by machine translation)
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Paragraph 0030; 0031; 0032
(2017/03/14)
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