- 1H, 13C, 2D NMR and GCMS characterization of diol derivatives
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Sodium borohydride (SBH) reduction of isocoumarins has been effected in presence of methanol to their respective diols. Diols have been isolated, purified and characterized by GCMS, proton, carbon and two-dimensional NMR spectroscopy analysis. Complete NMR assignments of diols are made using H-H COSY, as well as HSQC, HMQC and HMBC heteronuclear correlation techniques.
- Manivel,Khan, F. Nawaz
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experimental part
p. 825 - 832
(2009/12/24)
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