Synthesis and Stereochemistry of 2,5-Dimethoxy 3,6-Disubstituted 1,4-Dioxanes Obtained from α-Hydroxy Dimethyl Acetals
Several α-hydroxy dimethyl acetals were shown to undergo bimolecular loss of CH3OH under acid catalysis to yield the corresponding 1,4-dioxane.In the case of the 3,3-dimethoxy-2-pentanol (5) rearrangement accounts for the formation of 3,6-diethyl-2,5-dime
Moriarty, Robert M.,Hou, Kwang-Chung
p. 4581 - 4583
(2007/10/02)
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