Pentafluorophenyl Esters for the Temporary Protection of the α-Carboxy Group in Solid Phase Glycopeptide Synthesis
The pentafluorophenyl ester of fluoren-9-ylmethoxycarbonyl serine was found to be stable to glycosylation conditions and the purified glycosylation product was easily incorporated into a solid phase assembly of a nonapeptide analogue of the antifreeze gly
Synthesis of Glycosyltyrosine Building Blocks for Solid-Phase Glycopeptide Assembly: Use of Aryl tert-Butyl Ethers as Glycosyl Acceptors in Aromatic Glycosylations
The synthesis of the suitably protected building blocks for solid-phase glycopeptide synthesis, Nα-Fmoc-Tyr(Bz4-β-D-Gal)-OPfp 3, Nα-Fmoc-Tyr(Bz4-α-D-Gal)-OPfp 4, Nα-Fmoc-Tyr(Bz3-α-L-Rha)-OPfp 6, Nα-Fmoc-TyrBz3-
Vargas-Berenguel, Antonio,Meldal, Morten,Paulsen, Hans,Jensen, Knud J.,Bock, Klaus
p. 3287 - 3294
(2007/10/02)
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