Air-Induced Disulfenylation of Alkenes: Facile Synthesis of Vicinal Dithioethers
A novel disulfenylation of alkenes with thiophenols and their corresponding disulfides by using air as the oxidant has been achieved. This transformation provides a facile and practical protocol for the synthesis of vicinal dithioethers under mild conditions.
The disulfidation reactions of alkenes with disulfides were thoroughly investigated in this paper. Using H2O or DCE as the solvent, most reactions occurred smoothly to give the corresponding disulfidated products in good to high yields at room temperature within 12 h.
Wang, Xiu-Ren,Chen, Fan
experimental part
p. 4547 - 4551
(2011/07/08)
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