The reaction of red phosphorus with 1-bromonaphthalene in the KOH-DMSO system: Synthesis of tri(1-naphthyl)phosphane
Red phosphorus reacts with 1-bromonaphthalene in the KOH-DMSO system upon heating (47-70°C, 3 h) to give tri(1-naphthyl)phosphane in 10% yield. Microwave activation (600 W, 6 min) of the reaction affords the above-mentioned phosphane in 25% yield.
Kuimov, Vladimir A.,Malysheva, Svetlana F.,Gusarova, Nina K.,Vakul'Skaya, Tamara I.,Khutsishvili, Spartak S.,Trofimov, Boris A.
experimental part
p. 198 - 203
(2011/10/08)
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