Efficient synthesis of p-bis-(chlorodifluoromethyl)benzene
Selective, high yield partial fluorination of p-bis-(trichloromethyl)benzene to p-bis-(chlorodifluoromethyl)benzene has been accomplished by warming a slurry of the p-bis-(trichloromethyl)benzene in anhydrous HF which also contains a small quantity of inert solvent, such as 1,2-dichloroethane.
Dolbier Jr., William R.,Duan, Jian-Xin,Rong, Xiao X.
p. 1091 - 1093
(2008/02/08)
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