Unexpected Pathway of the High-Pressure Reaction Between 2-Methylfuran and Alkyl Glyoxylates
High-pressure reactions of 2-methylfuran with activated carbonyl compounds, n-butyl and (R)-menthyl glyoxylate are described.The reactions carried out in toluene under 11 kbar at 50 deg C afforded ca 1:1 mixtures of two regioisomeric products 4 and 5, which after benzylation were separated by column chromatography.
Jurczak, Janusz,Belniak, Stanislaw,Kozluk, Tomasz
p. 271 - 274
(2007/10/02)
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