cas 15474-96-1, CHLOROACETYL-GLYCYL-GLYCINE | Articles data ｜lookchem

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15474-96-1

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Conversion of Dipeptides and a Tetrapeptide to Macrocyclic Ionophores by means of Caesium Aided Ring Closure of the N-2-Chloroacetyl Derivatives
Three di-, (Gly)2, (Val)2 and (Leu)2, and one tetrapeptide, (Gly)4, have been acylated with 2-chloroacetyl chloride and the resulting products treated with Cs2CO3 in the dimethylformamide (DMF) solution; (Gly)2 and (Leu)2 provided strained 9-membered rings whereas (Val)2 dimerized to the 18-membered ring.
Kruizinga, Wim H.,Kingma, Rob,Leegstra, Libbe,Rokaszewski, Edward,Gruppen, Gert,Kellogg, Richard M.
p. 1647 - 1648
(2007/10/02)

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Chemical Properties

Melting Point: 179 °C
Boiling Point: 618°Cat760mmHg
Flash Point:327.6°C
Density: 1.434g/cm³
Solubility:very faint turbidity in hot Methanol
Vapor Pressure: 7.3E-17mmHg at 25°C
PKA: 3.27±0.10(Predicted)
PSA: 95.50000
LogP: -0.67600

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