cas 155155-64-9, METHYL (PHENYL 5-ACETAMIDO-4,7,8,9-TETRA-O-ACETYL-3,5-DIDEOXY-2-THIO-D-GLYCERO-D-GALACTO-2-NONULOPYRANOSID)ONATE | Articles data ｜lookchem

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155155-64-9

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Synthesis of N,N-Ac,Boc laurylthio sialoside and its application to O-sialylation
The combination of the 5-N-tert-butoxycarbonyl (Boc) group of laurylthio sialoside and cyclopentyl methyl ether (CPME) as a solvent enhanced the reactivity and α-selectivity of the sialyl donor during sialylation. Selective deprotection of the N-Boc group
Ikeda, Kiyoshi,Miyamoto, Keisuke,Sato, Masayuki
p. 7431 - 7435
(2007)
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Synthesis of thio- and selenoglycosides by cleavage of dichalconides in the presence of zinc/zinc chloride and reaction with glycosyl bromides
A convenient odorless methodology has been devised for the preparation of 1,2-trans-thio- and selenoglycosides through zinc-mediated cleavage of disulfides and diselenides and reaction of the thiolate and selenides formed in situ with glycosyl bromides. T
Mukherjee, Chinmoy,Tiwari, Pallavi,Misra, Anup Kumar
p. 441 - 445
(2007/10/03)

Approaches to intramolecular sialylation 2. * Synthesis of per-O-acetylated thioglycosides of N-acetylneuraminic acid containing an unprotected carboxy group
Various approaches to the synthesis of per-O-acetylated thioglycosides of N-acetylneuraminic acid (Neu5Ac) containing an unprotected carboxy group starting from the corresponding methyl esters were comparatively studied. One-step demethylation of methyl t
Kononov,Shpirt,Ito,Ogawa
p. 1442 - 1446
(2007/10/03)

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Chemical Properties

Melting Point: 183 °C
Boiling Point: 670.995oC at 760 mmHg
Flash Point:359.605oC
Density: 1.329g/cm3
Solubility:soluble in Chloroform
Storage Temp.:Freezer
Vapor Pressure: 0mmHg at 25°C
Refractive Index: -121 ° (C=1, CHCl3)
PKA: 13.79±0.70(Predicted)
PSA: 195.13000
LogP: 1.69070

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