cas 15811-32-2, 2-Fluoro-2',3',5'-triacetoxyadenosine | Articles data ｜lookchem

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15811-32-2

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Nucleic acid related compounds. 34. Non-aqueous diazotization with tert-butyl nitrite. Introduction of fluorine, chlorine, and bromine at C-2 of purine nucleosides
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Robins,Uznanski
p. 2608 - 2611
(1981)
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The preparative method for 2-fluoroadenosine synthesis
The preparative method for the synthesis of 2-fluoroadenosine starting from commercially available guanosine was developed. It included the intermediate formation of 2-amino-6-azido-9-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl) purine, which was isolated exclu
Berzin,Dorofeeva,Leonov,Miroshnikov
experimental part
p. 193 - 196
(2010/04/29)

Process for the preparation of fludarabine or fludarabine phosphate from guanosine
A process for the production of fludarabine or fludarabine phosphate is provided, wherein the nucleoside guanosine or a suitable derivative is employed as the starting material. The guanosine starting material is subjected to (a) conversion of the 6-keto group into a 6-amino group, (b) conversion of the 2-amino group to a 2-fluoro group, and (c) conversion of the ribofuranosyl moiety to an arabinofuranosyl moiety. Steps (a), (b), and (c) can be performed individually or concomitantly and in any sequence.
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(2008/06/13)

Process for the production of 2-fluoropurine derivatives
This invention relates to a process for the production of 2-fluoropurine derivatives from 2-aminopurine derivatives, which are reacted in HF/pyridine or HF/pyridine/H2 O in the presence of a nitrite.
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(2008/06/13)

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Chemical Properties

Melting Point: 194-197 ºC
Boiling Point: 635.4 ºC at 760 mmHg
Flash Point:338.1 ºC
Density: 1.684 g/cm³
Storage Temp.:Keep in dark place,Inert atmosphere,Room temperature
PKA: 1.30±0.10(Predicted)
PSA: 157.75000
LogP: 0.45270

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