- Method for synthesize aryltris (tri-R-siloxanyl) silane
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The invention relates to the technical field of organic chemistry. In order to solve the problem of complex steps in the process of synthesizing aryltris (tri-R-siloxanyl) silane,the invention provides a method for synthesizing aryltris (tri-R-siloxanyl) silane. An organic solvent is used as solvent, trialkylsilane and hydrogen peroxide react for 1-2 hours, then triethylamine and aryltrichlorosilane are respectively added, and the mixture is allowed to react for 1-5 hours, organic phase is filtered and concentrated to obtain aryltris (tri-R-siloxanyl) silane. The method adopts one pot reaction, which has the advantages of mild conditions, high yield and high product purity, and the process is simple.
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Paragraph 0027; 0028
(2019/01/08)
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