Efficient synthesis of mono- and diarylphosphinic acids: a microwave-assisted palladium-catalyzed cross-coupling of aryl halides with phosphinate
A general, efficient method for the microwave-assisted synthesis of mono- and diarylphosphinic acids from anilinium phosphinate and aryl halides, using Pd(0) and Xantphos as a supporting ligand, was developed.
Kalek, Marcin,Stawinski, Jacek
experimental part
p. 10406 - 10412
(2010/02/27)
New syntheses of arylphosphinic acids from the reaction of ethyl diethoxymethylphosphinate with aryl bromides and phenols
The chemistry of the hypophosphorous acid synthon, ethyl diethoxymethylphosphinate 1 has been further developed to afford efficient new routes to arylphosphinic acids 6 and 2-hydroxyphenylphosphinic acids 10.In one approach, a palladium(0) catalysed P-H i
Bennett, Stuart N. L.,Hall, Roger G.
p. 1145 - 1152
(2007/10/02)
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