cas 2517-07-9, methylenecyclopropylglycine | Articles data ｜lookchem

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2517-07-9

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Synthesis of (±)-(2-methylenecyclopropyl)glycine and (±)-4-[amino(carboxymethyl)]spiro[2.2]pentane-1-carboxylie acid
A facile method for the preparation of racemic cyclopropylglycines is described, involving oxidation of cyclopropylcarbinols followed by a Bucherer-Berg reaction with sequential hydrolysis of the hydantoins obtained. Georg Thieme Verlag Stuttgart.
Averina, Elena B.,Yashin, Nikolai V.,Grishin, Yurii K.,Kuznetsova, Tamara S.,Zefirov, Nikolai S.
p. 880 - 884
(2007/10/03)

THE PALLADIUM(II)-ASSISTED SYNTHESES OF (+)-Α-(METHYLENECYCLOPROPYL) GLYCENE AND (+)-TRANS-α-(CARBOXYCYCLOPROPYL) GLYCINE, TWO BIOACTIVE AMINO ACIDS.
Title compounds 1 and 2 have been synthesized efficiently from β-hydroxyallylglycine derivative 3 via the Pd(II)-catalyzed reactions.
Kurokawa, Natsuko,Ohfune, Yasufumi
p. 83 - 84
(2007/10/02)

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Chemical Properties

Melting Point: 246 °C (decomp)
Boiling Point: 309°Cat760mmHg
Flash Point:140.7°C
Density: 1.18g/cm³
Solubility:Chloroform (Slightly), DMSO (Slightly), Water (Slightly)
Storage Temp.:Amber Vial, -20°C Freezer, Under inert atmosphere
Vapor Pressure: 0.00471mmHg at 25°C
PKA: 2.18±0.10(Predicted)
PSA: 49.33000
LogP: 0.72760

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