cas 25384-14-9, 2'-AMINOACETOPHENONE HYDROCHLORIDE | Articles data ｜lookchem

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25384-14-9

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Selective and Additive-Free Hydrogenation of Nitroarenes Mediated by a DMSO-Tagged Molecular Cobalt Corrole Catalyst
We report on the first cobalt corrole that effectively mediates the homogeneous hydrogenation of structurally diverse nitroarenes to afford the corresponding amines. The given catalyst is easily assembled prior to use from 4-tert-butylbenzaldehyde and pyrrole followed by metalation of the resulting corrole macrocycle with cobalt(II) acetate. The thus-prepared complex is self-contained in that the hydrogenation protocol is free from the requirement for adding any auxiliary reagent to elicit the catalytic activity of the applied metal complex. Moreover, a containment system is not required for the assembly of the hydrogenation reaction set-up as both the autoclave and the reaction vessels are readily charged under a regular laboratory atmosphere.
Sch?fberger, Wolfgang,Timelthaler, Daniel,Topf, Christoph
supporting information
p. 2114 - 2120
(2021/07/22)

Efficient dibenzo[c]acridine helicene-like synthesis and resolution: Scaleup, structural control, and high chiroptical properties
Herein, we describe our recent expeditious synthesis of dibenzo[c]acridine helicene-like compounds on a large scale in pure enantiomeric form. This flexible synthesis allows for variation at several positions on the skeleton. Geometrical parameters related to these compounds have been obtained from monocrystal X-ray structure resolution. Additionally, chiroptical parameters have been recorded, highlighting the versatility of this family showing for example optical rotation at 589 nm varying between 135 and 150 deg g -1cm2.
Jierry, Loic,Harthong, Steven,Aronica, Christophe,Mulatier, Jean-Christophe,Guy, Laure,Guy, Stephan
supporting information; experimental part
p. 288 - 291
(2012/03/22)

Steric Acceleration by Ortho Substituents of the Stannous Chloride Reduction of Nitrobenzenes in Aqueous Ethanol
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Xing, Wen-Kan,Ogata, Yoshiro
p. 3577 - 3581
(2007/10/02)

Synthesis and properties of 6H [1]benzopyrano[4,3 b] quinoleines and 6H [1]benzothiapyrano[4,3 b] quinoleines
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Jacquignon,Croisy,Ricci,Balucani
p. 3862 - 3871
(2007/10/04)

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Chemical Properties

Melting Point: 285-289 °C(lit.)
Boiling Point: 251.8 °C at 760 mmHg
Flash Point:106.1 °C
Storage Temp.:Inert atmosphere,Room Temperature
PSA: 43.09000
LogP: 2.85460

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