Methylhydrazinium nitrate was synthesized by the reaction of dilute nitric acid with methylhydrazine in water and in methanol.The white needles formed are extremely hygroscopic and melt at 37.5-40.5 deg C.The IR spectrum differs from that reported elsewhere.The mass spectrum exhibited no parent peak at 109 m/z and thermogravimetric analysis indicated that the compound decomposed slowly at 63-103 deg C to give ammonium and methylammonium nitrate.The density is near 1.55 g/cm3.
Lawton, Emil A.,Moran, Clifford M.
p. 357 - 358
(2007/10/02)
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