cas 30315-46-9, (S)-3-tert-Butylamino-1,2-propanediol | Articles data ｜lookchem

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30315-46-9

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A Strategy for the Transformation of a Multifunctional Chiral Synthon of Moderate ee into an Enantiomerically Pure Synthetic Intermediate
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D'Arrigo, Paola,Feliciotti, Luca,Pedrocchi-Fantoni, Giuseppe,Servi, Stefano
p. 6394 - 6396
(2007/10/03)

(4S)-4-tert-Butylaminomethyl-2-Phenyl-1,3-Dioxolanes, the By-Products in the Synthesis of (5S)-2-Phenyl-3-terf-Butyl-5-Hydroxymethyloxazolidines
Condensation of (S)-(-)-3-tert-butylamino-1,2-propanediol with benzaldehyde in the presence of benzoic acid yielded predominantly (2S,4S)- and (2R,4S)-2-phenyl-4-tert-butylaminomethyl-1,3-dioxolanes along with the usual reaction products, (5S)-2-phenyl-3-tert-butyl-5-hydroxymethyloxazolidines.
Bredikhin,Novikova,Bredikhina
p. 378 - 380
(2007/10/03)

Stereoselective synthesis of the β2-adrenergic blocking agent IPS 339 from optically active precursors
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Leclerc,Amlaiky,Rouot
p. 69 - 74
(2007/10/02)

Synthesis of the β adrenergic blocking agent timolol from optically active precursors
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Weinstock,Mulvey,Tull
p. 3121 - 3124
(2007/10/05)

1-SUBSTITUTED AMINO-3-THIENO-[3,2-c]PYRIDINYLOXY-2-PROPANOLS
This invention provides new compounds of formula I, STR1 wherein X is sulphur or oxygen,R is alkyl of 3 to 7 carbon atoms or cycloalkyl of 3 to 7 carbon atoms, cycloalkyl of 3 to 7 carbon atoms monosubstituted by alkyl of 1 to 4 carbon atoms, α-dialkylpropinyl of 5 to 9 carbon atoms or α-dialkyl-allyl of 5 to 9 carbon atoms, hydroxyalkyl of 2 to 7 carbon atoms or phenoxyalkyl of 8 to 11 carbon atoms, the oxygen atom of the last two radicals being separated by at least two carbon atoms from the nitrogen atom to which R is bound, R 1 isI. hydrogen or alkyl of 1 to 4 carbon atoms in the 2,3,6 or 7 position, orIi. chlorine or bromine, in the 2, 3 or 7 position,Iii. nitro or--NHA wherein A is alkanoyl of 1 to 4 carbon atoms, in the 2, 3 or 7 position, orIv. fluorine, cyano or COOB, wherein B is alkyl of 1 to 4 carbon atoms, in the 2 or 3 position, andR 2 isI. hydrogen or alkyl of 1 to 4 carbon atoms in the 2, 3, 6 or 7 position,Ii. chlorine or bromine, in the 2, 3 or 7 position, orIii. fluorine in the 2 or 3 position,Useful in the treatment of heart diseases.
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(2008/06/13)

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Chemical Properties

Appearance/Colour :white flakes or powder
Melting Point: 85-89 °C(lit.)
Boiling Point: 262.4 °C at 760 mmHg
Flash Point:109.1 °C
Density: 0.992 g/cm³
Solubility:Chloroform, DMSO, Methanol
Storage Temp.:Keep in dark place,Inert atmosphere,Room temperature
Vapor Pressure: 0.00155mmHg at 25°C
Refractive Index: -29 ° (C=2, 1mol/L HCl)
PKA: 14.06±0.20(Predicted)
PSA: 52.49000
LogP: 0.11860

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