cas 31106-82-8, 2-(Bromomethyl)pyridine hydrobromide | Articles data ｜lookchem

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31106-82-8

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Optically pure heterobimetallic helicates from self-assembly and click strategies
Single diastereomer, diamagnetic, octahedral Fe(ii) tris chelate complexes are synthesised that contain three pendant pyridine proligands pre-organised for coordination to a second metal. They bind Cu(i) and Ag(i) with coordination geometry depending on the identity of the metal and the detail of the ligand structure, but for example homohelical (ΔFe, ΔCu) configured systems with unusual trigonal planar Cu cations are formed exclusively in solution as shown by VT-NMR and supported by DFT calculations. Similar heterobimetallic tris(triazole) complexes are synthesised via clean CuAAC reactions at a tris(alkynyl) complex, although here the configurations of the two metals differ (ΔFe, ΛCu), leading to the first optically pure heterohelicates. A second series of Fe complexes perform less well in either strategy as a result of lack of preorganisation.
Howson, Suzanne E.,Clarkson, Guy J.,Faulkner, Alan D.,Kaner, Rebecca A.,Whitmore, Michael J.,Scott, Peter
p. 14967 - 14981
(2013/10/22)

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Chemical Properties

Appearance/Colour :A pale-yellow to brown crystalline powder
Melting Point: 149-152 ºC
Boiling Point: 201.7°Cat760mmHg
Flash Point:75.8°C
Density: 1.533g/cm³
Solubility:soluble in Methanol
Storage Temp.:Keep in dark place,Sealed in dry,Room Temperature
Vapor Pressure: 0.433mmHg at 25°C
PSA: 12.89000
LogP: 2.93460

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