cas 3180-78-7, 1-(β-D-Glucopyranosyl)-5-methylpyrimidine-2,4(1H,3H)-dione | Articles data ｜lookchem

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3180-78-7

Articles about 3180-78-7Total 7 be found

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Visser et al.
p. 1926
(1948)
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Miles
p. 2565,2566
(1957)
Read Online

SELECTIVE VALORIZATION OF BIOMASS SUGARS
Disclosed are methods of forming an epimer or a dehydrated isomer of a pyranose monosaccharide or a pyranose saccharide residue in an oligosaccharide or a glycoside.
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Page/Page column 23; 31-32

(2021/06/26)

Synthesis of pyranonucleoside-6′-triphosphates through the cyclosal-method
The high yielding synthesis of pyranonucleoside-6′-triphosphates by using the cycloSal-method is described. Synthesis of the activated cycloSal-pyranonucleoside-6′-phosphate triesters was achieved by applying a synthetic route that had been developed for the synthesis of cycloSal-(glycopyranosyl-6)-phosphates by us. The route involved regioselective 6′-tert-butyldimethylsilyl protection and exchange of the silyl protecting group by the fluorenylmethyloxycarbonyl (Fmoc) group. The 6′-Fmoc- protected derivatives were selectively converted into the cycloSal-triester. These were then very efficiently converted into triphosphates by a "titration-like" reaction with pyrophosphate. Simple purification by first ion exchange followed by reversed phase (RP) column chromatography afforded the triphosphates in very good yields. Copyright
Huchting, Johanna,Meier, Chris
p. 3423 - 3429
(2014/06/09)

Oligodeoxyribonucleosides containing 1-β-D-glucopyranosylthymine: Synthesis and substrate properties
Regioselective method for 1-β-D-glucopyranosylthymine incorporation into oligonucleotides has been developed and substrate properties of the latters in DNA synthesis and hydrolysis reactions were investigated.
Ermolinsky, Boris S.,Fomitcheva, Marina V.,Efimtseva, Ekaterina,Meshkov, Sergey E.,Mikhailov, Sergey N.,Esipov, Dmitriy S.,Boldyreva, Elena F.,Korobko, Vyacheslav G.
p. 1619 - 1634
(2007/10/03)

The action of diethylaminosulfur trifluoride (DAST) on 1-(4,6-O-isopropylidene-β-D-glucopyranosyl)pyrimidines, a one-pot synthesis of 2,2'-anhydro-1-(3-deoxy-3-fluoro-4,6-O-isopropylidene-β-D-altropyranosyl)pyrimidines
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Leclerq, Francoise,Antonakis, Kostas
p. 277 - 282
(2007/10/02)

Stereospecific Vorbrueggen-like Reactions of 1,2-Anhydro Sugars. An Alternative Route to the Synthesis of Nucleosides
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Chow, Ken,Danishefsky, Samuel
p. 4211 - 4214
(2007/10/02)

Synthesis of thymine nucleosides over silyl-pyrimidine-binding
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Wittenburg
p. 1095 - 1114
(2007/10/04)

A NEW SYNTHETIC METHOD OF NUCLEOSIDES.
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NISHIMURA,SHIMIZU,IWAI
p. 1470 - 1472
(2007/10/04)

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Chemical Properties

Melting Point: 271 °C
Boiling Point: °Cat760mmHg
Flash Point:°C
Density: 1.614g/cm³
PKA: 9.57±0.10(Predicted)
PSA: 145.01000
LogP: -3.18260

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