cas 38767-72-5, 4-AMINO-PYRIDIN-2-OL | Articles data ｜lookchem

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38767-72-5

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Concise Entries to 4-Halo-2-pyridones and 3-Bromo-4-halo-2-pyridones
Methods for the synthesis of both simple 4-halo-2-pyridones and more functionalized 3,4-di- and (3,4,5-tri)-halo-2-pyridones are described that are based on a combination of Sandmeyer and regioselective (copper-mediated) halogenation, with a 2-chloro or a 2-benzyloxy moiety serving as a masked 2-pyridone.
Honraedt, Aurélien,Gallagher, Timothy
supporting information
p. 67 - 69
(2015/12/26)

Synthesis of the analogue nucleoside 3-deaza-2'-deoxycytidine and its template activity with DNA polymerase
A new synthesis of the nucleoside analogue 3-deaza-2'-deoxycytidine is described. The N3-nitrogen of dC is involved in the central hydrogen bond of a dG-dC base pair. The relative importance of hydrogen bonding as a controlling factor in the activity of DNA polymerase is examined by studying both duplex stability and template effects for this dc3C nucleoside. Duplexes containing dG-dc3C base pairs were strongly destabilized while templates containing the analogue nucleoside were found to incorporate only the complementary dG triphosphate, similar to observations with templates containing the native 2'-deoxycytidine.
Searls, Tim,McLaughlin, Larry W.
p. 11985 - 11996
(2007/10/03)

A General Route to 5- and 6-Substituted 4-Amino-2-oxo-1,2-dihydropyridines
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Nguyen Chi Hung,Bisagni, Emile
p. 765 - 766
(2007/10/02)

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Chemical Properties

Melting Point: 219-221 °C(Solv: acetone (67-64-1))
Boiling Point: 310.7 °C at 760 mmHg
Flash Point:141.7 °C
Density: 1.208 g/cm³
Storage Temp.:under inert gas (nitrogen or Argon) at 2–8 °C
PKA: 11.49±0.10(Predicted)
PSA: 59.14000
LogP: 0.95060

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