cas 395-68-6, 4-NITRO-2-(TRIFLUOROMETHYL)ACETANILIDE | Articles data ｜lookchem

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395-68-6

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Preparation 2-trifluoromethyl-4-substituted aniline compounds
The invention relates to a method for preparing 2-trifluoromethyl-4-substituted phenylamine and 2-trifluoromethyl-4-substituted acetanilide. The method for preparing the2-trifluoromethyl-4-substituted phenylamine and 2-trifluoromethyl-4-substituted acetanilide comprises the following main step: in the presence of sodium trifluoromethanesulfonate and tert-butyl hydroperoxide but no metal salt catalyst and under the stirring condition, maintaining a 4-substituted phenylamine compound (concrete structure shown in a formula II is described in the specification) in a reaction medium of mixture composed of dichloromethane and water at the temperature of 0-25 DEG C for 72-120 hours, so that the 2-trifluoromethyl-4-substituted phenylamine target product is obtained. The preparation method provided by the invention has potential commercial value.
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Paragraph 0023-0026; 0077-0080

(2017/02/23)

Copper-free direct C-H trifluoromethylation of acetanilides with sodium trifluoromethanesulfinate
A copper-free direct C-H ortho trifluoromethylation of electron-deficient 4-substituted acetanilides using Langlois reagent (NaSO2CF3) as the CF3 source in the presence of tert-butyl hydroperoxide (tBuOOH, TBHP) was developed.
Wu, Mingxi,Ji, Xinfei,Dai, Wenpeng,Cao, Song
p. 8984 - 8989
(2015/01/09)

Diaminopuridine-containing thiourea inhibitors of herpes viruses
Compounds of the formula STR1 are useful in the treatment of diseases associated with herpes viruses including human cytomegalovirus, herpes simplex viruses, Epstein-Barr virus, varicella-zoster virus, human herpesviruses-6 and -7, and Kaposi herpesvirus.
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(2008/06/13)

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Chemical Properties

Melting Point: 146-150 °C
Boiling Point: 371.8 °C at 760 mmHg
Flash Point:178.7 °C
Density: 1.478 g/cm³
Vapor Pressure: 1.01E-05mmHg at 25°C
Refractive Index: 1.532
PSA: 74.92000
LogP: 3.16820

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