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423-60-9

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A Lewis acid catalytic process for preparing fluorocarboxylic acid halides
Selected Group III and Group V Lewis acids were found to catalyze the isomerization and rearrangement of halosulfonyldifluoromethyl group (Rf-CF2SO2X, where X is either chlorine or fluorine) to form fluorocarboxylic acid halides (RfCOX). Fluorodesulfoxylation of the halosulfonyldifluoromethyl group yielded SOF2 as one of the two sulfur-containing oxides. Product analysis would suggest that both Lewis acid catalyzed and halogen exchange reactions are occurring and are dependent upon the starting halosulfonyldifluoromethyl material and Lewis acid.
Behr,Cheburkov
p. 369 - 372
(2007/10/03)

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Chemical Properties

Melting Point: 36 °C
Boiling Point: 188.5 °C at 760 mmHg
Flash Point:67.8 °C
Density: 1.813 g/cm³
Solubility:Chloroform (Slightly), Ethyl Acetate (Slightly)
Storage Temp.:Refrigerator, under inert atmosphere
Vapor Pressure: 0.825mmHg at 25°C
Refractive Index: 1.308
PSA: 42.52000
LogP: 6.60270

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