cas 50924-49-7, Mizoribine | Articles data ｜lookchem

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50924-49-7

Articles about 50924-49-7Total 6 be found

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A novel synthesis of Mizoribine and related nucleosides from acyclic precursors
Mizoribine (4-carbamoyl-1-β-D-ribofuranosylimidazolium-5-olate)(13β) and its 4-cyano analogue (20) were synthesized by formation of a malonamide from 2,3-isopropylidene-D-ribosylamine and a malonic acid derivative followed by amination, cyclisation and deprotection steps.
Ewing,Humble,Mackenzie,Shaw
p. 369 - 372
(1995)
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Synthesis of bredinin from 5-aminoimidazole-4-carboxamide-ribofuranoside (AICA riboside)
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Fukukawa,Shuto,Hirano,Ueda
p. 1644 - 1646
(1984)
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A synthesis of bredinin (Mizoribine) from an acyclic precursor
Bredinin (4-carbamoyl-1-β-d-ribofuranosylimidazolium-5-olate, 1) was synthesised by the formation of a malonamate from 2,3-isopropylidene-d- ribofuranosylamine and ethyl malonyl chloride, followed by a sequence involving amination, via reduction of an oxime, heterocycle formation and then deprotection.
Humble, Robert W.,Middleton, Danielle F.,Banoub, Joseph,Ewing, David F.,Boa, Andrew N.,MacKenzie, Grahame
scheme or table
p. 6223 - 6227
(2011/12/14)

Process for producing mizoribine by Eupenicillium javanicum
The invention relates to a fermentation process for producing mizoribine which comprises cultivating a microorganism belonging to genus Eupenicillium.
-
(2008/06/13)

Synthesis of bredinin from 1-β-D-ribofuranosyl-5-aminoimidazole-4-carboxamide by a photo-reaction
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Fukukawa,Shuto,Hirano,Ueda
p. 3653 - 3657
(2007/10/02)

Studies on imidazole derivatives and related compounds. 4. Synthesis of O-glycosides of 4-carbamoylimidazolium-5-olate
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Tarumi,Takebayashi,Atsumi
p. 849 - 854
(2007/10/02)

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Chemical Properties

Appearance/Colour :Crystalline solid
Melting Point: >200 °C
Boiling Point: 755.9 °C at 760 mmHg
Flash Point:410.9 °C
Density: 2.06 g/cm³
Solubility:DMSO (Slightly), Water (Slightly)
Storage Temp.:2-8°C
Vapor Pressure: 5.2E-24mmHg at 25°C
Refractive Index: 1.794
PKA: 6.75(at 25℃)
Merck: 14,6222
PSA: 151.06000
LogP: -2.00060

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