cas 5466-27-3, 4-ethoxycarbonyl-2-quinolone | Articles data ｜lookchem

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5466-27-3

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Microwave-assisted synthesis of quinoline derivatives from isatin
Microwave irradiation has been used for a rapid and efficient synthesis of quinoline-4-carboxylic acids 5a-g and 1,2,3,4-tetrahydroacridine-9-carboxylic acid (6) from the reaction of isatins 1-3 with acyclic and cyclic ketones in basic medium. 2-Hydroxyquinoline-4-carboxylic acid (11) was also obtained by irradiating a mixture of isatin 1 and malonic acid in AcOH. The esters of 5f and 11 and their respective hydrazides 8 and 13 were also prepared under MWI. Copyright Taylor & Francis, Inc.
El Ashry, El Sayed H.,Ramadan, El Sayed,Hamid, Hamida Abdel,Hagar, Mohamed
p. 2243 - 2250
(2007/10/03)

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Chemical Properties

Boiling Point: 421°C at 760 mmHg
Flash Point:208.4°C
Density: 1.246g/cm³
Vapor Pressure: 2.7E-07mmHg at 25°C
PSA: 59.16000
LogP: 1.70480

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