The present invention relates to a general synthesis for producing secondaryalkoxy-1-alkenes in commercial quantities in good yields by reacting cyclic and acyclic ketones and the corresponding alcohol with a secondary alkyl orthoformate ester in the presence of an acid catalyst, a Lewis acid, ferric chloride being preferred, and recovering the produce as a liquid of high purity.
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(2008/06/13)
An efficient synthesis of ketone enol ethers mediated by N-(1-alkoxyalkyl)benzotriazoles
A new general method for the transformation of ketones into their enol ethers in good yield is developed via elimination of benzotriazole from N-(1-alkoxyalkyl)benzotriazole intermediates.
Katritzky,Bayyuk,Rachwal
p. 279 - 283
(2007/10/02)
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