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59293-67-3

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Nonenzymatic Dynamic Kinetic Resolution of in situ Generated Hemithioacetals: Access to 1,3-Disubstituted Phthalans
The first nonenzymatic DKR reaction of hemithioacetals is developed. Hemithioacetals were formed in situ via thiol addition and subsequently underwent an intramolecular oxa-Michael reaction. The scope of the reaction was quite broad ranging from aliphatic to aromatic substituents and 1,3-disubstituted-1,3-dihyroisobenzofuran products were obtained in good yields with moderate diastereoselectivities and high enantioselectivities. (Figure presented.).
Nath, Utpal,Chowdhury, Deepan,Pan, Subhas Chandra
p. 1628 - 1633
(2018/03/21)

One pot rapid synthesis of thiols from alcohols under mild conditions
Thiols are prepared in high yields from corresponding alcohols using Ph3P, NBS in acetone and followed by addition of polymer supported hydrosulfide under mild condition.
Bandgar,Sadavarte
p. 908 - 910
(2007/10/03)

Solid Supported Reagents and Reactions. Part 21.1 Rapid and Clean Synthesis of Thiols from Halides Using Polymer-supported Hydrosulfide
A variety of thiols are prepared from corresponding halides using polymer-supported hydrosulfide in excellent yields. Isolation of pure products by simple filtration and evaporation is an important feature of this method.
Bandgar, Babasaheb P.,Pawar, Sanjay B.
p. 212 - 213
(2007/10/03)

Carbamimidothioic acid phenylmethyl ester salts and their N,N'-tetramethyl derivatives as possible antimicrobial agents
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Tait,Di Bella,Bondi,Quaglio,Fabio
p. 617 - 630
(2007/10/02)

Sulfur-containing imidazoles
Novel imidazole mercaptals of the formula STR1 wherein each m is independently zero or one; and R1 and R2 each are independently selected from (lower)alkyl, cycloalkyl, cycloalkyl(lower)alkyl, phenyl, phenyl(lower)alkyl, thienyl, thienyl(lower)alkyl, pyridyl and pyridyl(lower)alkyl, in which the phenyl and heterocyclic rings optionally may contain from 1 to 3 substituents, and acid addition salts thereof, are useful antimicrobial agents.
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(2008/06/13)

Synthesis of certain derivatives of thiols.
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BOENIGK,CHRISTIAN,JENKINS
p. 357 - 360
(2007/10/06)

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Chemical Properties

Boiling Point: 150-151°C 12mm
Flash Point:150-151°C/12mm
Density: 1,36 g/cm3
Vapor Pressure: 0.0139mmHg at 25°C
Refractive Index: 1.6045
Sensitive: Air Sensitive
BRN: 509602
PSA: 38.80000
LogP: 3.42320

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