cas 60546-62-5, 6-BROMO-3,4-METHYLENEDIOXYBENZOIC ACID | Articles data ｜lookchem

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60546-62-5

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Regioselective ring opening by propanethiolate of (methylenedioxy)benzenes with electron-withdrawing substituents
The ring opening reaction of (methylenedioxy)benzenes 1 with propanethiolate in DMF leads to products 2 and/or 3, depending on the nature of the electron-withdrawing substituent Z.
Cassels, Bruce K.,Radetski, Claudemir,Rezende, Marcos Caroli
p. 448 - 450
(2007/10/02)

Cleavage of Methylenedioxy Ring. II. Cleavage with Sodium Phenoxide and Methoxide in Dimethyl Sulfoxide
Regioselective cleavage of the methylenedioxy ring in piperonals (1, 6, and 7) and 3,4-methylenedioxynitrobenzenes (8 and 9) by oxide ions in dimethyl sulfoxide was achieved: the 4-hydroxybenzene derivatives (2, 10-13, and 22) were obtained with the phenoxide ion, while the 3-hydroxybenzene derivatives (4, 18-21, 23, 26, and 29) were obtained with the methoxide or benzyloxide ion.Keywords - cleavage of methylenedioxy ring; regioselectivity; piperonals; 3,4-methylenedioxynitrobenzenes; sodium phenoxide; sodium methoxide; dimethyl sulfoxide; 3-hydroxybenzene derivatives; 4-hydroxybenzene derivatives; NMR spectra
Kobayashi, Shigeru,Imakura, Yasuhiro,Horikawa, Ritsuko
p. 1287 - 1293
(2007/10/02)

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Chemical Properties

Melting Point: 200-204 °C
Boiling Point: 358.9°Cat760mmHg
Flash Point:170.8°C
Density: 1.894g/cm³
Vapor Pressure: 8.93E-06mmHg at 25°C
PKA: 3.00±0.20(Predicted)
PSA: 55.76000
LogP: 1.87600

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