[60]Fullerene diol issued from pentaerythritol derivatives
A new [60]fullerene diol is synthesized in good yield, in two steps starting from reaction of C602- anion with the benzylideneacetal derived from 2,2-bis(iodomethyl)-1,3-propanediol. The corresponding [60]fullerene bis-mesylate is also formed in a similar way starting from bis-iodo bis-mesylate compound in the same series. The scope of this fullerene diol in synthesis is exemplified by its easy esterification with 4-formyl benzoyl chloride.
Chopin, Stéphanie,Delaunay, Jacques,Cousseau, Jack
Two possible versions of the synthesis of 5-iodo-methyl-5-chloromethyl- and 5,5-bis(iodomethyl)-1,3-dioxanes from 3,3-bis(chloromethyl)oxetane and aldehydes, differing in the sequence of the stages, were investigated.The 5-iodomethyl-5-chloromethyl- and 5
Kurmaeva, E. S.,Chalova, O. B.,Chistoedova, G. P.,Lapuka, L. F.,Kiladze, T. K.,et al.
p. 119 - 123
(2007/10/02)
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