cas 69491-56-1, 3-Pyrimidin-2-ylaniline | Articles data ｜lookchem

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69491-56-1

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Copper mediated C-H amination with oximes: En route to primary anilines
Here we report an efficient Cu(i)-mediated C-H amination reaction with oximes as amino donors to introduce NH2 groups directly. Various strongly coordinating heterocycles including quinoline, pyrimidine, pyrazine, pyrazole and triazole were tolerated well. The potential utility was further demonstrated in a late-stage modification of telmisartan (an antagonist for the angiotensin II receptor).
Xu, Lin-Lin,Wang, Xing,Ma, Biao,Yin, Ming-Xing,Lin, Hai-Xia,Dai, Hui-Xiong,Yu, Jin-Quan
p. 5160 - 5164
(2018/06/21)

BENZAMIDES AND NICOTINAMIDES AS SYK MODULATORS
The present invention is directed to compounds of formula I and pharmaceutically acceptable salts, esters, and prodrugs thereof which are inhibitors of Syk kinase. The present invention is also directed to intermediates used in making such compounds, the preparation of such a compound, pharmaceutical compositions containing such a compound, methods of inhibition Syk kinase activity, methods of inhibition the platelet aggregation, and methods to prevent or treat a number of conditions mediated at least in part by Syk kinase activity, such as Non Hodgkin's Lymphoma.
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Page/Page column 116

(2012/05/20)

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Chemical Properties

Melting Point: 99.5 °C
Boiling Point: 268.51 °C at 760 mmHg
Flash Point:140.346 °C
Density: 1.193 g/cm³
Vapor Pressure: 0.008mmHg at 25°C
Refractive Index: 1.634
PSA: 51.80000
LogP: 2.30700

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