Studies on Aconitum species. XV. Deoxygenation reaction of aconitine type alkaloids
Mesaconitine (1) in tetrahydrofuran reacted with sodium hydride, a catalytic amount of imidazole, carbon disulfide and methyl iodide at room temperature to give the di-O-(S-methyl)thiocarbonate (5). The reductive cleavage of 5 with tri-n-butyltin hydride
Mori,Murayama,Bando,Kawahara
p. 2803 - 2806
(2007/10/02)
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