- Process for the preparation of tertiary butyl hydrazine hydrohalogenide
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An industrially and economically advantageous process for the preparation of a TBH-HX using starting materials which are cheaply available and are easy to handle, maintaining a high yield. A tertiary butyl hydrazine hydrohalogenide is prepared by reacting a hydrazine hydrohalogenide with a methyl tertiary butyl ether in the presence of an acid.
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- 1,1,4,4,-TETRAALKYLAMIDAZINES. SYNTHESIS OF MONOALKYLHYDRAZINES
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A series of 1,1,4,4,-tetraalkylamidazines were synthesized.Their IR, UV, and 1H and 13C NMR spectra were investigated, and the characteristics of their stereochemical structure are discussed.Amidazines are alkylated by the action of alkyl iodides at the imine nitrogen atom.Alkaline cleavage of the alkyl iodide derivatives is a method for the production of monoalkylhydrazines.
- Zelenin, K. N.,Khrustalev, V. A.,Sergutina, V. P.
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p. 244 - 247
(2007/10/02)
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