Single-stage synthesis of alkyl-H-phosphinic acids from elemental phosphorus and alkyl bromides
Elemental phosphorus (red or white) reacts with alkyl bromides at 60–62 °C in the phase-transfer catalytic system KOH/H2O/PhMe/Et3BnNCl to afford alkyl-H-phosphinic acids in up to 47% yield.
Gusarova, Nina K.,Sutyrina, Anastasiya O.,Kuimov, Vladimir A.,Malysheva, Svetlana F.,Belogorlova, Natalia A.,Volkov, Pavel A.,Trofimov, Boris A.
p. 328 - 330
(2019/06/13)
Effect of electrolysis conditions on the process of anodic oxidation of tertiary phosphines in the presence of camphene
Anodic oxidation of tertiary phosphines (Et3P, Pr3P, Bu3P, i-Bu3P and Am3P) in the presence of camphene and heterogenic base (trisodium phosphate) on platinum anode in acetonitrile solution of sodium
Zagumennov, V. A.,Sizova, N. A.
p. 1368 - 1373,6
(2020/09/16)
Conversion of Thio- And Selenophosphoryl into Phosphoryl Group by Perfluoro cis-2,3-Dialkyloxaziridines
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Arnone, Alberto,Novo, Barbara,Pregnolato, Massimo,Resnati, Giuseppe,Terreni, Marco
p. 6401 - 6403
(2007/10/03)
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