Ketalization of Dihydroxy Sulfones (8-S-4 Species) by Cyclodehydration To Form Spirobicyclic Oxysulfurane Oxides (10-S-5 Species)
Dihydroxy sulfones 6 and 7 react with the dehydrating agent Ph2S(OC(CF3)2Ph)2 (1) to give sulfurane oxides 8 and 9, respectively.These reactions are thought to be the first examples of direct ketalization of sulfones by dehydration.A possible mechanism fo
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