METHOD FOR PREPARING GLYCIDYLOXYSTYRENE MONOMERS AND POLYMERS THEREOF
It was found that glycidyloxystyrenes, including glycidyloxystyrene and substituted glycidyloxystyrene, can be synthesized from hydroxycinnamic acid or substituted hydroxycinnamic acids in a one-pot, two-step process. The substrate can be thermally decarboxylated and then without purification, reacted in the presence of a halomethyl-oxirane and a base. The resulting product can be polymerized or coppolymerized to a fully substituted product.
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(2008/12/06)
Synthesis of trithiocarbonates
This invention provides an efficient method for synthesizing trithiocarbonates, RSC(S)SR′ that can be used, for example, as RAFT agents in the living polymerization of styrenics, acrylates, and other olefinic monomers.
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Page/Page column 1-2
(2010/11/27)
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