- An improved practical synthesis of leuco-1,4,5,8-tetrahydroxyanthraquinone
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Leuco-1,4,5,8-tetrahydroxyanthraquinone was prepared from chrysazin by nitration and reduction with iron powder, followed by treatment with sodium hydrosulfite in alkaline solution. This method is suitable for scaling, and is significant and improved over literature methods.
- Chang,Cheng
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p. 1893 - 1900
(2007/10/02)
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- An improved procedure for the preparation of 4,5-dinitrochrysazin
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Pure 4,5-dinitrochrysazin was prepared by selective nitration of chrysazin, followed by solvent extraction of impurities. This method is suitable for scaling without need of chromatography, and represents a significant improvement over literature methods.
- Chang
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p. 931 - 937
(2007/10/02)
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