The convergent total synthesis of brevetoxin B (1) has been achieved. The intramolecular allylation of the O,S-acetal 20, prepared from the α-chlorosulfide 17 and the alcohol 5, was carried out using AgOTf as a Lewis acid to give the diene 21, predominant
Synthesis of a multifunctional radioiodinatable photoaffinity probe
Synthesis is described which results in an iodinatable photoaffinity probe and derivatives which are useful in the covalent coupling of the probe to amine, carboxylic acid, and alcoholic hydroxy function on specific ligands of biological importance. Speci
Mende,Schulman,Baden
p. 5307 - 5310
(2007/10/02)
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