cas 857410-67-4, ETHYL 2-AMINO-6-METHYLPYRIMIDINE-4-CARBOXYLATE | Articles data ｜lookchem

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857410-67-4

Articles about 857410-67-4Total 1 be found

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Reaction of β-alkoxyvinyl α-ketoesters with acyclic NCN binucleophiles – Scalable approach to novel functionalized pyrimidines
Two protocols for synthesis of series of low-molecular-weight di- and tri-substituted pyrimidines bearing a functional group at the 4th position, which rely on a base-mediated condensation of amidines or guanidines with β-alkoxyvinyl α-keto esters, have been developed. This approach allowed for multigram preparation of novel pyrimidine-4-carboxylates in 21–90% yield. The synthetic utility of these compounds was demonstrated by some standard functional group transformations providing promising building blocks for organic synthesis and drug discovery.
Stepaniuk, Oleksandr O.,Rudenko, Tymofii V.,Vashchenko, Bohdan V.,Matvienko, Vitalii O.,Kondratov, Ivan S.,Tolmachev, Andrey A.,Grygorenko, Oleksandr O.
p. 3472 - 3478
(2019/05/17)

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Chemical Properties

Melting Point: 151 °C(Solv: ethanol (64-17-5))
Boiling Point: 368.4±34.0 °C(Predicted)
Density: 1.217±0.06 g/cm3(Predicted)
Storage Temp.:under inert gas (nitrogen or Argon) at 2–8 °C
PKA: 2.71±0.10(Predicted)
PSA: 78.83000
LogP: 0.47400

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