Process for the production of low flammability electrolyte solvents
The invention provides a method for producing electrolyte solvent, the method comprising reacting a glycol with a disilazane in the presence of a catalyst for a time and at a temperature to silylate the glycol, separating the catalyst from the silylated glycol, removing unreacted silazane; and purifying the silylated glycol.
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Page/Page column 6; 7
(2016/03/13)
Highly conductive trimethylsilyl oligo(ethylene oxide) electrolytes for energy storage applications
Monomethyl ethers of oligoethylene glycols with different chain lengths were converted to trimethylsilyl derivatives by reacting with trimethylchlorosilane in the presence of triethylamine, or by directly refluxing with excess trimethylchlorosilane or hex
Zhang, Lingzhi,Zhang, Zhengcheng,Harring, Scott,Straughan, Megan,Butorac, Rachel,Chen, Zonghai,Lyons, Leslie,Amine, Khalil,West, Robert
experimental part
p. 3713 - 3717
(2010/03/01)
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