cas 88069-49-2, Pilsicainide hydrochloride

The present invention relates to a method for manufacturing a pyrrolizidine compound and a method for manufacturing pyrrolizidine hydrochloride hemihydrate. According to the present invention, by including the reaction using phosphoryl chloride (POCl_3) and pyridine, and also aniline intermediates, it is possible to provide effects of lowering the manufacturing cost of the pyrrolizidine compound and pyrrolizidine hydrochloride hemihydrate, solving the manufacturing environmental problem, and at the same time, increasing a manufacturing yield.

The invention discloses a preparation method of pilsicainide hydrochloride. The preparation method comprises the following steps of: by taking 2, 6-dimethylaniline as a raw material, carrying out amidation reaction on the 2, 6-dimethylaniline and a compou

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88069-49-2

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Chemical Properties

Melting Point: 212-214°

Boiling Point: 416.9 °C at 760 mmHg

Flash Point:205.9 °C

Solubility:Chloroform (Slightly), Water (Slightly)

Storage Temp.:room temp

Vapor Pressure: 3.7E-07mmHg at 25°C

PSA: 32.34000

LogP: 3.27130

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