Organophosphorus Chemistry. III. Synthesis of 3-Ethoxy-2-phenyl-1,3-azaphosphininane 3-Oxide
Treatment of ethyl (3-bromopropyl)phosphonochloridate with benzylmagnesium chloride gave ethyl (benzyl)(3-bromopropyl)phosphinate.This underwent free-radical bromination to give ethyl (α-bromobenzyl)(3-bromopropyl)phosphinate.Cyclization with aqueous ammo
Hewitt, David G.,Teese, Murray W.
p. 205 - 210
(2007/10/02)
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