Synthesis of 3,5-Disubstituted and 3,4,5-Trisubstituted λ3-Phosphorins from 1-tert-Butyl-1,6-dihydro-3(2H)-phosphorinones
5-Aryl-1-tert-butyl-1,6-dihydro-3(2H)-phosphorinones 13 - easily available by reduction of the phosphane oxides 1 with phenylsilane - react with 1 mol of RMgX (RLi) exclusively by formation of the enolates, however with 6 mol of RMgX (RLi), after reaction
Maerkl, Gottfried,Hock, Klaus,Merz, Loni
p. 763 - 782
(2007/10/02)
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