cas 942-97-2, 2-(4-METHOXY-2-METHYLPHENYL)ACETIC ACID | Articles data ｜lookchem

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942-97-2

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Carboxylation of benzylic and aliphatic C-H bonds with CO2 induced by light/ketone/nickel
A photoinduced carboxylation reaction of benzylic and aliphatic C-H bonds with CO2 is developed. Toluene derivatives capture gaseous CO2 at the benzylic position to produce phenylacetic acid derivatives when irradiated with UV light in the presence of an aromatic ketone, a nickel complex, and potassium tert-butoxide. Cyclohexane reacts with CO2 to furnish cyclohexanecar-boxylic acid under analogous reaction conditions. The present photoinduced carboxylation reaction provides a direct access from readily available hydrocarbons to the corresponding carboxylic acids with one carbon extension.
Ishida, Naoki,Masuda, Yusuke,Imamura, Yuuya,Yamazaki, Katsushi,Murakami, Masahiro
supporting information
p. 19611 - 19615
(2019/12/24)

Synthesis of 4-Hydroxy-2-methylbenzoic Acid and Its Higher Homologues
Synthesis of 4-hydroxy-2-methylbenzoic acid (1a) and its higher homologues such as 4-hydroxy-2-methylphenylacetic acid (1b), 3-(4-hydroxy-2-methylphenyl)propanoic acid (1c) and 4-(4-hydroxy-2-methylphenyl)butanoic acid (1d) are described.
Sen, P. K.,Pal, Panchanan,Goswami, Shyamaprosad,Chattopadhyay, Gautam
p. 679 - 682
(2007/10/02)

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Chemical Properties

Boiling Point: 327.8oC at 760 mmHg
Flash Point:130.2oC
Density: 1.146g/cm3
Storage Temp.:Sealed in dry,Room Temperature
Vapor Pressure: 8E-05mmHg at 25°C
PSA: 46.53000
LogP: 1.63070

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