cas 95061-47-5, (R)-(+)-2-HYDROXY-1,2,2-TRIPHENYLETHYL ACETATE | Articles data ｜lookchem

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95061-47-5

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A chiral synthesis of (-)-spiro[1-azabicyclo[2.2.2]octane-3,5′- oxazolidin-2′-one]: A conformationally restricted analogue of acetylcholine that is a potent and selective α7 nicotinic receptor agonist
A direct, short chiral synthesis of the selective α7 nicotinic receptor agonist (-)-spiro[1-azabicyclo[2.2.2]-octane-3,5′-oxazolidin- 2′-one] (AR-R17779) is presented. The key step utilized attack of the dianion of the (R)-HYTRA ester [(R)-(+)-2-hydroxy-1,2,2-triphenylethyl acetate] on quinuclidin-3-one, followed by a selective precipitation of the diasteriomeric tertiary alcohol that led to (S)-(-)-AR-R17779 in two additional steps.
Macor, John E.,Mullen, George,Verhoest, Patrick,Sampognaro, Anthony,Shepardson, Bruce,Mack, Robert A.
p. 6493 - 6495
(2007/10/03)

(R)-(+)-2-hydroxy-1,2,2-triphenylethyl acetate [ 1,2-ethanediol, 1,1,2-triphenyl-, 2-acetate, (R)- ]
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Macor, John,Sampognaro, Anthony J.,Verhoest, Patrick R.,Mack, Robert A.,Gaul, Christoph,Martin, Stephen F.
p. 45 - 45
(2017/09/08)

Stereoselective Aldol Reactions with (R)- and (S)-2-Hydroxy-1,2,2-triphenylethyl Acetate and Related Glycol Monoacetates
The enolate 7a, formed by double deprotonation of the ester 5a, is added to aldehydes.The influences of the enolate gegenion, of the solvent, and of the reaction temperature on the ratio of the isomeric products 9:10 are studied.The highest degrees of dia
Devant, Ralf,Mahler, Ulrike,Braun, Manfred
p. 397 - 406
(2007/10/02)

(R)- AND (S)-2-ACETOXY-1,1,2-TRIPHENYLETHANOL - EFFECTIVE SYNTHETIC EQUIVALENTS OF A CHIRAL ACETATE ENOLATE
The enolate 3, easily available by double deprotonation of (R)-2-acetoxy-1,1,2-triphenylethanol (5), adds in a highly stereoselective manner to aldehides.Hydrolysis of the adducts 6/7 affods the acids 2.
Braun, Manfred,Devant, Ralf
p. 5031 - 5034
(2007/10/02)

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Chemical Properties

Appearance/Colour :white to light yellow crystal powder
Melting Point: 237-240 °C(lit.)
Boiling Point: 487.647 °C at 760 mmHg
Flash Point:197.557 °C
Density: 1.18 g/cm³
Storage Temp.:Store below +30°C.
Vapor Pressure: 2.53E-10mmHg at 25°C
Refractive Index: 1.603
PKA: 12.40±0.29(Predicted)
PSA: 46.53000
LogP: 4.22690

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