Unexpected silicon group transfer in difunctional alkoxy silanes
During the hydrosilylation reaction of a difunctional silane with allyl glycidyl ether (AGE), two scrambled hydrosilylation products were produced in significant amounts. This scrambling is reaction condition dependent and has been observed in a few other examples. It appears to be the first such alkoxysilane transformation to occur under these conditions, although similar siloxane transformations have been documented. This also introduces a method of preparing certain organofunctional alkyldialkoxysilanes in high purities via hydrosilylation, where the close boiling rearrangement by-products are minimized.
Filipkowski, Michelle A.,Petty, Herbert E.,Westmeyer, Mark D.,Schilling Jr., Curtis L.
p. 15 - 19
(2013/09/06)
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